Detector calibration procedure for detectors with a single axis goniostat.

 

What is needed?

Well diffracting, single Lysozyme crystal, preferably frozen; 50-90 images, 1 degree oscillation, diffraction to the detector edge.

When the sample-detector distance is motor controlled, two data sets with two different distances should be collected.

When the detector has the ability to collect data with 2theta offset, two additional data sets with swing angle 5 degree and -10 degree should be also collected.