Detector calibration procedure for detectors with a single axis goniostat.

 

What is needed?

Well-diffracting, single Lysozyme crystal, preferably frozen; 50-90 images, 1-degree oscillation [0.1 degrees for HPC detectors], diffraction to the detector edge.

When the sample-detector distance is motor controlled, two data sets with two different distances should be collected.

When the detector has the ability to collect data with 2theta offset, two additional data sets with a swing angle of 5 degrees and -10 degrees should be also collected.